5,5-二甲己烷2,4-二酮合成路线 (共 27 条)
参考文献
Bulletin de la Societe Chimique de France, , p. C 27, C 29
Bulletin de la Societe Chimique de France, , p. 946,948
参考文献
Kutz; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 4040
反应条件
ozone T=-15°C; Behandeln des Reaktionsprodukts mit Wasser;
参考文献
Weygand; Baumgaertel
Chemische Berichte, 1929 , vol. 62, p. 579
参考文献
Kutz; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 4040
反应条件
T=60 - 100°C; P=110326 - 147102 Torr; Hydrogenation;
参考文献
Sprague; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 2669,2671
参考文献
Kutz; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 4040
参考文献
Kutz; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 4040
反应条件
4-methyl-3-nitrobenzenesulfonyl azide; triethylamine in dichloromethane T=20°C;
参考文献
Zakharova, Valerija M.; Hennig, Lothar; Nikolaev, Valerij A.
Synthesis, 2005 , # 17 art. no. T16204SS, p. 2871 - 2874
反应条件
1: Raney nickel; methanol / 100 °C / Hydrogenation.unter Druck 2: oxalic acid / Durch Destillation 3: Raney nickel / 30 - 40 °C / 73550.8 Torr / Hydrogenation View Scheme
参考文献
Stutsman; Adkins
Journal of the American Chemical Society, 1939 , vol. 61, p. 3306
参考文献
Kutz; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 4040