74497-02-2合成路线 （共 11739 条）
反应条件
2: H2SO4
3: conc. HCl / Heating
4: 80 percent / toluene / 240 h / Heating
5: 95 percent / LiAlH4 / tetrahydrofuran; CH2Cl2 / Ambient temperature
View Scheme
参考文献
Colapret; Diamantidis; Spencer; Spaulding; Rudo
Journal of Medicinal Chemistry, 1989 , vol. 32, # 5 p. 968 - 974
参考文献
Simonov, V. D.; Chernova, L. N.; Akhmerova, S. G.; Yasman, Ya. B.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1974 - 1978
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 11 p. 2313 - 2318
反应条件
1: ethanol / |Reflux
2: lithium tert-butylate; 4-toluenesulfonyl azide / dichloromethane / 20 °C
View Scheme
参考文献
Cheng, Guolin; Zeng, Xiaobao; Shen, Jinhai; Wang, Xuesong; Cui, Xiuling
Angewandte Chemie - International Edition, 2013 , vol. 52, # 50 p. 13265 - 13268
Angew. Chem., 2013
反应条件
iodine; tetra-n-butylphosphonium iodide; praseodymium(III) trifluoromethanesulfonate
T=160°C; 36 h; Inert atmosphere;
参考文献
Yin, Peng; Loh, Teck-Peng
Organic Letters, 2009 , vol. 11, # 17 p. 3791 - 3793
反应条件
acetic acid; zinc in water
T=60 - 70°C; 4 h;
参考文献
Micovic; Ivanovic; Piatak; Bojic
Synthesis, 1991 , # 11 p. 1043 - 1045
参考文献
Loevenich et al.
Chemische Berichte, 1929 , vol. 62, p. 3095
反应条件
in acetonitrile
T=65°C; Rate constantMechanism;
参考文献
Oh, Hyuck Keun; Kwon, Young Bong; Cho, In Ho; Lee, Ikchoon
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1697 - 1702
反应条件
in acetonitrile
T=65°C; Rate constantMechanism;
参考文献
Oh, Hyuck Keun; Kwon, Young Bong; Cho, In Ho; Lee, Ikchoon
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1697 - 1702
反应条件
triphenylphosphine
T=60°C; 1 h; neat (no solvent);
参考文献
Jafari, Abbas Ali; Nazarpour, Mahshid; Abdollahi-Alibeik, Mohammad
Heteroatom Chemistry, 2010 , vol. 21, # 6 p. 397 - 403
反应条件
tantalum pentachloride in dichloromethane
T=20°C; 24 h;
参考文献
Chandrasekhar; Prakash, S. Jaya; Jagadeshwar; Narsihmulu, Ch
Tetrahedron Letters, 2001 , vol. 42, # 32 p. 5561 - 5563
