in neat (no solvent) mixt. of metal and I2 was heated to the deflagration point of the mixt. in vac.; excess of I2 was evacuated, tube was filled with Ar, solidified metal part was removed, elem. anal.; metal triiodide was deposited on the wall of tube;
参考文献
Khoroshenkov; Petrovskaya; Fedushkin; Bochkarev
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 3 p. 699 - 702
in tetrahydrofuran (N2); molar ratio of Gd:I2 2:3; clear THF soln. of triiodide obtained by filtration or decanting;
参考文献
Goryushkin, V. F.; Poshevneva, A. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1992 , vol. 37, p. 994 - 995
Zhurnal Neorganicheskoi Khimii, 1992 , vol. 37, p. 1928 - 1931
in neat (no solvent) mixt. of metal and I2 was heated to the deflagration point of the mixt. in vac.; excess of I2 was evacuated, tube was filled with Ar, solidified metal part was removed, elem. anal.; metal triiodide was deposited on the wall of tube;
参考文献
Khoroshenkov; Petrovskaya; Fedushkin; Bochkarev
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 3 p. 699 - 702
