反应条件
in neat (no solvent)
Kinetics; byproducts: N2, CO2; mixing of stoich. amts. of Na2CO3, NaNO3 and Ni3S2 in porcelain mortar, placing in a stainless steel boat, covering with lid, placing in muffle furnace preheated to 300-700°C, heating at this temp. for 1-60 min; cooling, crushing, leaching with H2O at 60°C for 40 min, filtration, drying, monitoring by XRD;
参考文献
Bogorodskii; Rybkin; Barankevich
Russian Journal of Inorganic Chemistry, 2011 , vol. 56, # 6 p. 831 - 834
