反应条件
in neat (no solvent) argon atmosphere; KI and org. compd. addn. to PCl4AlCl4 (cooling), reaction vessel connecting to vac. line (2 mm Hg), mixt. heating to 80°C, liquefaction; volatiles collection (trap cooled with liq. nitrogen);
参考文献
Vengel'nikova, V. N.; Timokhin, B. V.; Kalabina, A. V.; Donskikh, V. I.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 1160 - 1163
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 1318 - 1322
