1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
1: Ambient temperature
2: 1) sodium hydride / 1) mineral oil, tetrahydrofuran, 50 deg C, 2) tetrahydrofuran, 50 deg C, overnight
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参考文献
Jones Jr.; Schnettler; Huber
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 3 p. 511 - 518
参考文献
Cromwell; Witt
Journal of the American Chemical Society, 1943 , vol. 65, p. 308,310
参考文献
Shell Devel. Co.
Patent: US2569132 , 1948 ;
反应条件
1: KNH2
2: polyphosphoric acid
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参考文献
Hauser; Harris
Journal of the American Chemical Society, 1958 , vol. 80, p. 6360,6363
反应条件
(i) NaH, LDA, THF, (ii) aq. HCl; Multistep reaction;
参考文献
Murray,T.P.; Harris,T.M.
Journal of the American Chemical Society, 1972 , vol. 94, p. 8253 - 8255
反应条件
T=100°C; 1 h; also with solvent, other time and temperature; Product distribution;
参考文献
Wendelin, Winfried; Schermanz; Karl; Schweiger, Klaus; Fuchsgruber, Alfred
Monatshefte fuer Chemie, 1983 , vol. 114, p. 1371 - 1380
反应条件
N-ethyl-N,N-diisopropylamine in methanol; hexane; acetonitrile
15 h; Ambient temperature;
参考文献
Aoyama, Toyohiko; Terasawa, Satomi; Sudo, Kimio; Shioiri, Takayuki
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, p. 3759 - 3760
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gompper, Rudolf; Vogt, Hans-Hubert
Chemische Berichte, 1981 , vol. 114, # 8 p. 2866 - 2883
参考文献
Claisen
Chemische Berichte, 1926 , vol. 59, p. 151
Full Text Show Details
Weygand
Chemische Berichte, 1925 , vol. 58, p. 1478
参考文献
Claisen
Chemische Berichte, 1926 , vol. 59, p. 151
Full Text Show Details
Weygand
Chemische Berichte, 1925 , vol. 58, p. 1478
