1,2,4,5-四氯苯合成路线 (共 206 条)
参考文献
Silberrad
Journal of the Chemical Society, 1922 , vol. 121, p. 1019
反应条件
methanesulfonic acid; nitrogen(IV) oxide; ozone in dichloromethane T=0 - 5°C; 10 h;
参考文献
Synthesis, , # 8 p. 841 - 845
参考文献
Justus Liebigs Annalen der Chemie, , vol. 192, p. 230
Annales de Chimie (Cachan, France), , vol. <4> 15, p. 257
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, , p. 347
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 10, p. 333
Justus Liebigs Annalen der Chemie, , vol. 192, p. 236
参考文献
Justus Liebigs Annalen der Chemie, , vol. 192, p. 230
反应条件
tetrabutylammomium bromide in N,N-dimethyl-formamide T=-5 - 0°C; Dehalogenation; Carboxylation; Electrochemical reaction; Further byproducts given;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 65, # 6 p. 862 - 880
反应条件
C42H44Cl3N3Pd; caesium carbonate in toluene; tert-butyl alcohol T=80°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Tu, Tao; Sun, Zheming; Fang, Weiwei; Xu, Mizhi; Zhou, Yunfei
Organic Letters, 2012 , vol. 14, # 16 p. 4250 - 4253
反应条件
1-[2-(diphenylphosphino)phenyl]ethanol; bis(acetylacetonate)nickel(II) in diethyl ether T=45°C; 96 h;
参考文献
Yoshikai, Naohiko; Mashima, Hiroko; Nakamura, Eiichi
Journal of the American Chemical Society, 2005 , vol. 127, # 51 p. 17978 - 17979
反应条件
NiF2; methylmagnesium bromide; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in tetrahydrofuran T=0 - 80°C; 27 h; Inert atmosphere;
参考文献
Hatakeyama, Takuji; Hashimoto, Sigma; Ishizuka, Kentaro; Nakamura, Masaharu
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11949 - 11963
反应条件
potassium hydroxide; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride; palladium diacetate in 1,4-dioxane T=95°C; Suzuki coupling;
参考文献
Burukin; Vasil'Ev; Merkulova; Chizhov; Mistryukov; Zlotin
Russian Chemical Bulletin, 2007 , vol. 56, # 7 p. 1467 - 1469
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium (II) trifluoroacetate; 18-crown-6 ether; potassium carbonate in supercritical carbon dioxide T=110°C; Suzuki-Miyaura reaction; P=82508.3 Torr; 18 h;
参考文献
Kuchurov, Ilya V.; Vasil'Ev, Andrei A.; Zlotin, Sergei G.
Mendeleev Communications, 2010 , vol. 20, # 3 p. 140 - 142