in dichloromethane
Ar-atmosphere; equimolar amts.; addn. of mixt. of SCl2 and SO2Cl2 to amide at -78°C, stirring overnight with warming to room temp.; filtration, evapn., recrystn. (PhMe);
参考文献
Maaninen, Arto; Laitinen, Risto S.; Chivers, Tristram; Pakkanen, Tapani A.
Inorganic Chemistry, 1999 , vol. 38, p. 3450 - 3454