2-亚甲基环己烷-1-醇合成路线 （共 70 条）
反应条件
biphenyl; naphthalenyl-1-carbonitrile in water; acetonitrile
Irradiation; Product distribution;
参考文献
Gassman, Paul G.; Bottorff, Kyle J.
Tetrahedron Letters, 1987 , vol. 28, # 45 p. 5449 - 5452
参考文献
Dreiding; Hartman
Journal of the American Chemical Society, 1953 , vol. 75, p. 939,940
反应条件
potassium hydroxide
T=110°C; multistep reaction; kinetic curves of expenditure and formation of corresponding allyl alcohols;
参考文献
Trofimov, B. A.; Petrova, O. V.; Vasil'tsov, A. M.; Mikhaleva, A. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 7.2 p. 1450 - 1453
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 7 p. 1601 - 1605
反应条件
Candida antarctica lipase B in tetrahydrofuran; hexane
T=50°C; 1.5 h; Resolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Tomin, Anna; Hornyanszky, Gabor; Kupai, Katalin; Dorko, Zsanett; Uerge, Laszlo; Darvas, Ferenc; Poppe, Laszlo
Process Biochemistry, 2010 , vol. 45, # 6 p. 859 - 865
反应条件
Candida antarctica lipase B in tetrahydrofuran; hexane
T=20°C; 1.5 h; Resolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Tomin, Anna; Hornyanszky, Gabor; Kupai, Katalin; Dorko, Zsanett; Uerge, Laszlo; Darvas, Ferenc; Poppe, Laszlo
Process Biochemistry, 2010 , vol. 45, # 6 p. 859 - 865
反应条件
hydrogen; cationic chelate biphosphine rhodium in dichloromethane
T=20°C; P=760 Torr;
参考文献
Brown, John M.; Hall, Stephen A.
Tetrahedron Letters, 1984 , vol. 25, # 13 p. 1393 - 1396
反应条件
RhH2(PPh3)4
T=175°C; 0.5 h; various metall complex catalysts; Product distribution;
参考文献
Felfoeldi, K.; Bartok, M.
Journal of Organometallic Chemistry, 1985 , vol. 297, p. C37 - C40
反应条件
(i) H2, Pt, (ii) CrO3, aq. AcOH; Multistep reaction;
参考文献
Stapleford,K.S.J.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 2580 - 2582
参考文献
Dreiding; Hartman
Journal of the American Chemical Society, 1956 , vol. 78, p. 1216
反应条件
in tetrahydrofuran; hexane; ethyl acetate
参考文献
Merck Frosst Canada, Inc.
Patent: US4667055 A1, 1987 ;
