54509-73-8合成路线 （共 3623 条）
反应条件
carbon T=150°C; P=26618.1 Torr; 24 h; Sealed; Product distribution / selectivity;
参考文献
BRANDVOLD, Timothy A.
Patent: US2010/331568 A1, 2010 ;
Location in patent: Page/Page column 4 ;
反应条件
ozone T=21.9°C; P=730 Torr; effect of reagent ratio; Product distribution;
参考文献
Neeb; Horie; Moortgat
International Journal of Chemical Kinetics, 1996 , vol. 28, # 10 p. 721 - 730
反应条件
aluminium trichloride in dichloromethane T=-10°C; 0.25 h;
参考文献
Stjernlof; Gullme; Elebring; Andersson; Wikstrom; Lagerquist; Svensson; Ekman; Carlsson; Sundell
Journal of Medicinal Chemistry, 1993 , vol. 36, # 15 p. 2059 - 2065
反应条件
[Ir(μ-acac-O,O,C3)(acac-O,O)(acac-C3)]2 in n-heptane; water T=180°C; anti-Markovnikov addition; P=14701.5 Torr; 2 h;
参考文献
Matsumoto, Takaya; Taube, Douglas J.; Periana, Roy A.; Taube, Henry; Yoshida, Hajime
Journal of the American Chemical Society, 2000 , vol. 122, # 30 p. 7414 - 7415
反应条件
aluminium trichloride T=100 - 300°C; P=25742.8 Torr;
参考文献
Koppers Co.
Patent: US2428102 , 1946 ;
Full Text Show Details
Koppers Co
Chem.Abstr., 1948 , p. 928
反应条件
water; cesium nitrate; tungstophosphoric acid; water; mixture of, dried, tabletted T=85.6 - 165°C; P=2250.23 Torr; Gas phase; Product distribution / selectivity;
参考文献
EP1218331 B1, ;
Page 6 ;
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=40°C; P=562.556 Torr; 24 h; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2011/2284 A1, ;
Page/Page column 19 ;
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=40°C; P=750.075 Torr; 24 h; Inert atmosphereGreen chemistry; Pressure;
参考文献
Spekreijse, Jurjen; Le Notre, Jerome; Scott, Elinor L.; Sanders, Johan P. M.; Van Haveren, Jacco
Green Chemistry, 2012 , vol. 14, # 10 p. 2747 - 2751,5
反应条件
[1,3-bis(2-methylphenyl)-2-(imidazolidene)dichloro(phenylmethylene)(tricyclohexylphosphine)]ruthenium (II) T=60°C; P=7757.43 Torr; 4 h; Conversion of starting material;
参考文献
GENOMATICA, INC.
Patent: WO2009/45637 A2, 2009 ;
Location in patent: Page/Page column 44-47 ;
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium T=60°C; P=7757.43 Torr; 4 h; Conversion of starting material;
参考文献
WO2009/45637 A2, ;
Page/Page column 44-47 ;
