in neat (no solvent, solid phase)
reactants were ground in an agate mortar or in a "wiggle bug" type stainless steel ball vibrator for several minutes to one hour; extd. with CCl4, detected by IR;
参考文献
Fernandez, J.; Gonzalez, E.; Onnate, J. De; Lopez, R.; Navarro, E.
Journal of Solid State Chemistry, 1993 , vol. 107, p. 314 - 318